Ac-Lys
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Analytical Conditions:
Apparatus : Acquity UPLCTM (Waters)
Column : Develosil RPAQUEOUS (C30)
3μm, 2.0 X 100 mm (Nomura Chemilac)
Analyte : AQC-derivatized L-Lys
Inject volume : 7.5 μL
Flow rate : 0.25 mL/min
Mobile phase A :
4% CH3CN in 0.1M CH3COONH4 (pH6.0)
Mobile phase B :
60% CH3CN in 0.1M CH3COONH4 (pH6.0)
Detection : λex=250 nm, λem=395 nm
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